The regularities of formation of a phase structure and structures of a diffusion zone under compression of diffusive pairs Ni - Zr, Ft - Ti, Fe - Nb, and Fe - No are investigated by the methods of autoradiography, X-ray analysis, and raster submicroscopy. The experiments are executed in the interval of deformation speeds <$E epsilon dot~=~5~symbol Ш~5~cdot~10 sup 3~roman s sup -1> and the temperature range 300 - 1600 К. In the hard phase, derivations of supersaturated hard solutions of intermetallic compounds including nonstoichiometric ones are revealed. The synthesis of intermetallic compounds can be considered as a critical process developing after reaching the particular temperature and speeds of deformation.

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